1-Adamantanecarbonyl chloride → HCID 20437845, compound

HRID 1979992Notes

Reaction equation

HRID 1979992 reaction equation
[OH:1][CH2:2][CH2:3][C:4]1[C:5]2[N:6]([N:17]=[CH:18][N:19]=2)[C:7]([NH2:16])=[N:8][C:9]=1[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1.[C:20]12([C:30](Cl)=[O:31])[CH2:29][CH:24]3[CH2:25][CH:26]([CH2:28][CH:22]([CH2:23]3)[CH2:21]1)[CH2:27]2>>[C:20]12([C:30]([O:1][CH2:2][CH2:3][C:4]3[C:5]4[N:6]([N:17]=[CH:18][N:19]=4)[C:7]([NH2:16])=[N:8][C:9]=3[C:10]3[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=3)=[O:31])[CH2:27][CH:26]3[CH2:25][CH:24]([CH2:23][CH:22]([CH2:28]3)[CH2:21]1)[CH2:29]2

Participants

3

Reactant 2

HCID 989151-Adamantanecarbonyl chlorideHCID 175635Sc-36741

Product 1

HCID 20437845HCID 20437845, compound

Procedure

The title compound was prepared by the method of Example 2 using 2.5 g (0.01 mole) of the product compound of Example 1 and 2.0 g (0.01 mole) of 1-adamantanecarbonyl chloride, except that the solution was not divided before purification.

Workup

  1. customwas not divided before purification

Sources & evidence

ORD record
ord-68504e3b067c49c485ab088f8b2b8e01
Source dataset
uspto-grants-1984_11
Patent number
US04483987

Reaction notes

Loading…