HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-2-chloroisopropylbenzene → HCID 68561612, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-2-chloroisopropylbenzene | HCID 50997869 | — |
| Reactant | 3-(4-Tert-butylbenzyl)-[1,2,3]oxathiazolidine 2,2-dioxide | HCID 86613991 | — |
| Product | HCID 68561612 | HCID 68561612 | 42.2% |
Reaction Steps
The title compound was synthesized in analogy to example S6-C using 4-bromo-1-chloro-2-isopropylbenzene (120 mg, 0.51 mmol), and 3-(4-tert-butylbenzyl)-[1,2,3]oxathiazolidine 2,2-dioxide (138 mg, 0.51 mmol). The residue was purified by flash column chromatography to give the desired product (74 mg, 42%) as a light yellow oil. MS (ISP) 344.3 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07745477B2 |
| Source dataset | uspto-grants-2010_06 |
| ORD ID | ord-cedd3c82bee5421996ebad9f7280c1c8 |
| Source note | uspto-grants-2010_06 |