HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 13363448, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | 3-Chloro-2-methyl-1-propene | HCID 11241 | — |
| Reactant | HCID 20437446 | HCID 20437446 | — |
| Product | HCID 13363448 | HCID 13363448 | — |
Reaction Steps
To a solution of 16.0 g of N-methyl-N-chlorosulfenyl carbamoyl chloride in 100 ml of methylene chloride was added 12.0 g of methallyl chloride with stirring, at room temperature. On slight heating there was a spontaneous exotherm which raised the temperature of the reaction mixture to 39° C. On removal of the solvent under reduced pressure 19.6 g of oil was obtained, N25D 1.5379.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04485113 |
| Source dataset | uspto-grants-1984_11 |
| ORD ID | ord-75700897304d47278d0b98aa8a125ab5 |
| Source note | uspto-grants-1984_11 |