HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylthio-2-methylpropionaldoxime → 2-Methylthio-2-methylpropionaldehyde O-[N-methyl-N-(2-chloromethyl-2-propanesulfenyl)carbamoyl] oxime
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylthio-2-methylpropionaldoxime | HCID 15436 | — |
| Reactant | N-methyl-N-(2-chloromethyl-2-propanesulfenyl)carbamoyl chloride | HCID 13363447 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | 2-Methylthio-2-methylpropionaldehyde O-[N-methyl-N-(2-chloromethyl-2-propanesulfenyl)carbamoyl] oxime | HCID 54355570 | — |
Reaction Steps
Prepared as in Example I by reacting 2-methylthio-2-methylpropionaldoxime with N-methyl-N-(2-chloromethyl-2-propanesulfenyl)carbamoyl chloride in the presence of triethylamine as an acid acceptor. The product was isolated as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04485113 |
| Source dataset | uspto-grants-1984_11 |
| ORD ID | ord-cb56be9e95e94775b529a8b4e7f92598 |
| Source note | uspto-grants-1984_11 |