Ethyl Methacrylate → HCID 131714184, compound

HRID 1980217Notes

Reaction equation

HRID 1980217 reaction equation
[C:1]([O:6]CC)(=[O:5])[C:2]([CH3:4])=[CH2:3].[CH2:9]([O:11][CH:12]([O:15][CH2:16][CH3:17])[CH2:13]Br)[CH3:10]>>[CH2:9]([O:11][CH:12]([O:15][CH2:16][CH3:17])[CH2:13][CH:3]=[C:2]([CH3:4])[C:1]([O-:6])=[O:5])[CH3:10].[CH2:9]([O:11][CH:12]([O:15][CH2:16][CH3:17])[CH2:13][O:6][C:1](=[O:5])[C:2]([CH3:4])=[CH2:3])[CH3:10]

Participants

4

Reactant 2

HCID 7343Ethyl MethacrylateHCID 74852Ethane, 2-bromo-1,1-diethoxy-

Product 2

HCID 212536982,2-Diethoxyethyl 2-methylprop-2-enoateHCID 131714184HCID 131714184, compoundYield 29%

Procedure

Analysis indicated that fraction #1 was predominantly ethyl methacrylate. Fraction #2 was predominantly bromoacetaldehyde diethylacetal. Fraction #3 was the desired product, 2,2 diethoxy-ethyl-methacrylate (29% yield).

Sources & evidence

ORD record
ord-a9c89a0429694898817e8028222150a9
Source dataset
uspto-grants-1985_04
Patent number
US04508594

Reaction notes

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