Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | HCID 86739038 | HCID 86739038 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20402431 | HCID 20402431 | 94.4% |
Reaction Steps
A total of 155 g of 2-(isopropylamino)propoxyethanol, 122 g of 37% aqueous formaldehyde, 5 g of 10% Pd/C and 1 l of methanol were charged to an autoclave, pressured to 1000 psi with H2 and heated at 80° C. for 3 hours. Filtration and distillation of the reaction mixture yielded 159 g of 2-(N-isopropyl-N-methylamino)propoxyethanol with b.p. of 125° C. at 20 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04508692 |
|---|
| Source dataset | uspto-grants-1985_04 |
|---|
| ORD ID | ord-f3de4fd0c7274c51b8149d271ab4d692 |
|---|
| Source note | uspto-grants-1985_04 |
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