HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorobenzoyl isocyanate → 1-(2-Chlorobenzoyl)-3-(5-(4-chlorophenyl)-2-pyridyl)urea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorobenzoyl isocyanate | HCID 9942311 | — |
| Reactant | 5-(4-Chlorophenyl)pyridin-2-amine | HCID 13242644 | — |
| Product | 1-(2-Chlorobenzoyl)-3-(5-(4-chlorophenyl)-2-pyridyl)urea | HCID 13242647 | — |
Reaction Steps
5-(4-Chlorophenyl)-2-pyridylamine (0.6 gram) and 2-chlorobenzoyl isocyanate (0.7 gram) were reacted according to the teaching of Example 7. The identity of the product was confirmed by NMR, yield 920 mg, m.p. 228°-231° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04508722 |
| Source dataset | uspto-grants-1985_04 |
| ORD ID | ord-6944b280585d46ce8fd61e6666967561 |
| Source note | uspto-grants-1985_04 |