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HRID1980312

反应详情

EQUATION

反应方程式

HRID 1980312 的结构方程式

REACTANTS

反应物

2
结构：O=C=NC(=O)c1c(Cl)cccc1Cl
HCID12912739

2,6-Dichlorobenzoyl isocyanate

C8H3Cl2NO2

结构：Cc1nc(N)ccc1-c1ccccc1
HCID13502855

6-Methyl-5-phenylpyridin-2-amine

C12H12N2

PRODUCTS

生成物

1
结构：Cc1nc(NC(=O)NC(=O)c2c(Cl)cccc2Cl)ccc1-c1ccccc1
HCID13242650

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

2,6-Dichlorobenzoyl isocyanate (650 mg) was reacted with 6-methyl-5-phenyl-2-pyridylamine (500 mg) in 25 ml of ethyl acetate. A precipitate formed which was filtered and confirmed by NMR as the desired product, 219°-220° C.

WORKUP

后处理

  1. customA precipitate formed which
  2. filtrationwas filtered
  3. customconfirmed by NMR as the desired product, 219°-220° C.