反应详情

温度

60 °C

52.25 g of 5,5-dichloro-3,3-dimethyl-pentanoic acid are reacted with 150 ml of thionyl chloride, first at room temperature and thereafter while warming at 60° C. By working up the mixture by distillation, 56.5 g of 5,5-dichloro-3,3-dimethyl-pentanoic acid-chloride of boiling point 114°-115° C./15 are obtained.

1. distillationby distillation, 56.5 g of 5,5-dichloro-3,3-dimethyl-pentanoic acid-chloride of boiling point 114°-115° C./15
2. customare obtained