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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1980375Generated: October 30, 2026

Thionyl Chloride → 5,5-Dichloro-3,3-dimethyl-pentanoic acid-chloride

https://huagongshe.com/reaction/1980375

Reaction equation

Participants

RoleNameHCIDCharge
ReactantThionyl ChlorideHCID 24386—
Reactant5,5-Dichloro-3,3-dimethylpentanoic acidHCID 20225909—
Product5,5-Dichloro-3,3-dimethyl-pentanoic acid-chlorideHCID 53996835—

Reaction Conditions

Temperature60 °C

Reaction Steps

52.25 g of 5,5-dichloro-3,3-dimethyl-pentanoic acid are reacted with 150 ml of thionyl chloride, first at room temperature and thereafter while warming at 60° C. By working up the mixture by distillation, 56.5 g of 5,5-dichloro-3,3-dimethyl-pentanoic acid-chloride of boiling point 114°-115° C./15 are obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04508913
Source datasetuspto-grants-1985_04
ORD IDord-f77c6cd585d3422ab1e353300d37547b
Source noteuspto-grants-1985_04