2-Chlorobenzoic Acid → HCID 20262575, compound

HRID 1980492Notes

Reaction equation

HRID 1980492 reaction equation
Cl[C:2]1[CH:10]=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=[O:5].[CH2:11]([O:18][C:19]1[CH:20]=[C:21]([CH:23]=[CH:24][CH:25]=1)[NH2:22])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>>[CH2:11]([O:18][C:19]1[CH:20]=[C:21]([NH:22][C:2]2[CH:10]=[CH:9][CH:8]=[CH:7][C:3]=2[C:4]([OH:6])=[O:5])[CH:23]=[CH:24][CH:25]=1)[C:12]1[CH:13]=[CH:14][CH:15]=[CH:16][CH:17]=1

Participants

3

Reactant 2

HCID 83742-Chlorobenzoic AcidHCID 928923-Benzyloxyaniline

Product 1

HCID 20262575HCID 20262575, compound

Procedure

2-(3-Benzyloxyphenylamino)benzoic acid [VII; R and R"=H, OR°=3--OCH2C6H5 ] was prepared from 2-chlorobenzoic acid and 3-benzyloxyaniline according to the procedure of Example 1(a). The green solid obtained was used directly in the next reaction.

Workup

  1. customThe green solid obtained
  2. customwas used directly in the next reaction

Sources & evidence

ORD record
ord-893f5d1a013e4d0c9db32ca1b9e99e2f
Source dataset
uspto-grants-1985_04
Patent number
US04510139

Reaction notes

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