HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenesulfonyl chloride → N-benzenesulfonyl-4-(2-bromoethyl) benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenesulfonyl chloride | HCID 7369 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 4-(2-Bromoethyl)benzenesulfonamide | HCID 14485091 | — |
| Product | N-benzenesulfonyl-4-(2-bromoethyl) benzenesulfonamide | HCID 54306985 | — |
Reaction Steps
As an additional variation of the reaction sequence, the 4-(2-bromoethyl) benzenesulfonamide produced as in Example I was reacted with benzenesulfonyl chloride and sodium hydroxide and then acidified to produce N-benzenesulfonyl-4-(2-bromoethyl) benzenesulfonamide. Recrystallization of a small portion from toluene gave a white solid, having a melting point of 148°-150° C. and a neutralization equivalent of 405 (theory 404).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04510324 |
| Source dataset | uspto-grants-1985_04 |
| ORD ID | ord-f192f9618b0c45879ad30df35d6ed0ae |
| Source note | uspto-grants-1985_04 |