Methylamine → HCID 178482523, compound

HRID 1980703Notes

Reaction equation

HRID 1980703 reaction equation
CO[C:3]1[C:7](OC)=[N:6][S:5](=[O:11])(=[O:10])[N:4]=1.[CH3:12][C:13]1[O:14][C:15]([CH2:18][S:19][CH2:20][CH2:21][NH2:22])=[N:16][N:17]=1.[CH3:23][NH2:24]>>[CH3:12][C:13]1[O:14][C:15]([CH2:18][S:19][CH2:20][CH2:21][NH:22][C:7]2[C:3]([NH:24][CH3:23])=[N:4][S:5](=[O:10])(=[O:11])[N:6]=2)=[N:16][N:17]=1

Participants

4

Reactant 3

HCID 6329MethylamineHCID 122305383,4-Dimethoxy-1,2,5-thiadiazole 1,1-dioxideHCID 15592303HCID 15592303, compound

Product 1

HCID 178482523HCID 178482523, compound

Procedure

When a suspension of 3,4-dimethoxy-1,2,5-thiadiazole 1,1-dioxide is treated with an equimolar amount of 2-[(2-methyl-1,3,4-oxadiazol-5-yl)methylthio]ethylamine [prepared in Step A] and an excess of methylamine by the general procedure described in Example 2, the title compound is thereby produced.

Sources & evidence

ORD record
ord-3d9527ad686641f09efbe638f9fd9ddd
Source dataset
uspto-grants-1985_04
Patent number
US04510309

Reaction notes

Loading…