HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Malonate → 5-(2,3-Dihydro-1,4-benzodioxin-6-yl)-3-hydroxycyclohex-2-en-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Malonate | HCID 7761 | — |
| Reactant | 4-(2,3-Dihydro-1,4-benzodioxin-6-yl)but-3-en-2-one | HCID 54150042 | — |
| Product | 5-(2,3-Dihydro-1,4-benzodioxin-6-yl)-3-hydroxycyclohex-2-en-1-one | HCID 13982937 | — |
Reaction Steps
5-(3,4-Ethylenedioxyphenyl)-3-hydroxycyclohex-2-en-1-one was prepared from 1-(3,4-ethylenedioxyphenyl)but-1-en-3-one and diethyl malonate following essentially the same procedure as that described in Example 1 part (ii). The product was obtained as a crystalline solid, mp 188° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04511391 |
| Source dataset | uspto-grants-1985_04 |
| ORD ID | ord-67c961ab95ed4b1b890ef0eaa530f082 |
| Source note | uspto-grants-1985_04 |