HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → HCID 20400701, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 20400735 | HCID 20400735 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20400701 | HCID 20400701 | — |
Reaction Steps
Add 23.1 gm of 2-chloro-5,6-dihydro-benzo[f]quinolin-3(4H)-one to 300 ml of methanol containing 30 gm of sodium methoxide. Heat the system in a steel bomb at about 200° C. for 12 hours. Stop the reaction, remove solvent, treat with water, and isolate the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04511569 |
| Source dataset | uspto-grants-1985_04 |
| ORD ID | ord-772c0c30718d4c30935a850f1538a678 |
| Source note | uspto-grants-1985_04 |