HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 20400796, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 20400817 | HCID 20400817 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 20400796 | HCID 20400796 | — |
Reaction Steps
A solution of 4 g of 3-(5-ethoxycarbonylpentyl)-1-methyl-2-(3-pyridyl)indole in 40 ml of n-butanol is saturated with methylamine and heated on a steam bath in a pressure bottle for 3 days. The reaction mixture is evaporated to dryness and the product is crystallized from ethyl-ether to yield the 3-[5-(N-methylcarbamoyl)pentyl]-1-methyl-2-(3-pyridyl)indole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04511573 |
| Source dataset | uspto-grants-1985_04 |
| ORD ID | ord-0e808f1f383d4e7698d89f7dd74a36a9 |
| Source note | uspto-grants-1985_04 |