HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosuccinimide → 1-(Chlorosulfanyl)-4-fluorobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | 4-Fluorothiophenol | HCID 67789 | — |
| Product | 1-(Chlorosulfanyl)-4-fluorobenzene | HCID 12669617 | 75.7% |
Reaction Steps
Employing the procedure of Example 13, p-fluorothiophenol (5.0 g., 39 mmoles) and N-chlorosuccinimide (5.2 g., 39 mmoles) were reacted to form p-fluorobenzenesulfenyl chloride (4.8 g., oil).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04511575 |
| Source dataset | uspto-grants-1985_04 |
| ORD ID | ord-733e2e743cda4ba39a5aa124059be6b3 |
| Source note | uspto-grants-1985_04 |