Diethyl Ether → HCID 13472124, compound

Participants

Reaction Steps

The 1-(6-dimethylaminohexanoyl)-1,2,3,4-tetrahydroquinoline (4.0 g) was added to a mixture of lithium aluminium hydride (1.4 g) and ether (200 ml). The mixture was refluxed for 5 hours, then cooled. Water was added cautiously, and the organic solution was separated, dried and evaporated to give the title compound as an oil which is then converted to the dihydrochloride, mp 116°-119°.

Provenance & Evidence