HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 20399850, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 70486795 | HCID 70486795 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20399850 | HCID 20399850 | — |
Reaction Steps
6-dimethylamino-1-(1,2,3,4-tetrahydroquinolin-1-yl)-hexane acetate (1.0 g) is dissolved in 50 ml water containing a stoichiometric equivalent of sulfuric acid, and the solution evaporated to dryness. The product is suspended in ethanol and filtered, air dried and recrystallized from methanol/acetone to yield 6-dimethylamino-1-(1,2,3,4-tetrahydroquinolin-1-yl)-hexane bisulfate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04512990 |
| Source dataset | uspto-grants-1985_04 |
| ORD ID | ord-a49692d0d02a4e75bdd19ec241475d79 |
| Source note | uspto-grants-1985_04 |