HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12750043, compound → HCID 12750037, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12750043 | HCID 12750043 | — |
| Solvent | Sodium Carbonate | HCID 10340 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 12750037 | HCID 12750037 | — |
Reaction Steps
A solution of methyl (Z)-6-phenyl-5-hexenoate (2.0 g) in dioxan (20 ml) and 10% sodium carbonate solution (20 ml) was heated under reflux for 6 hours and evaporated to low volume. The residue was diluted with water, washed with ether, acidified and extracted with ether. The extract was dried and evaporated to give (Z)-6-phenyl-5-hexenoic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04513005 |
| Source dataset | uspto-grants-1985_04 |
| ORD ID | ord-b23ebd1e3f9048e592eee332bc79c302 |
| Source note | uspto-grants-1985_04 |