HCID 13105361, compound → HCID 13105328, compound

Participants

Reaction Steps

A stirred solution of methyl (E)-8-phenyl-5-octenoate (13.6 g) in dioxan (125 ml) and 10% sodium carbonate solution (125 ml) was heated under reflux for 7 hours then evaporated. The residue in water was washed with ether, acidified and extracted with ether and the extract was dried and evaporated. The residue was distilled under vacuum to give the title compound, b.p. 150° to 153° C./0.2 mm.

Provenance & Evidence