Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | L-Proline benzyl ester hydrochloride | HCID 3084256 | — |
| Solvent | Water | HCID 962 | — |
| Product | Proline benzyl ester | HCID 99767 | 103% |
Reaction Steps
A mixture of 2.4 g of benzyl DL-prolinate hydrochloride, 25 ml of benzene, 5 ml of demineralized water and 1.01 g of triethylamine was stirred at 20° C. for one hour and the decanted organic phase was wahsed with water, dried and evaporated to dryness under reduced pressure to obtain 2.1 g of benzyl DL prolinate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04513139 |
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| Source dataset | uspto-grants-1985_04 |
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| ORD ID | ord-7d1473eefdf140a4a12d09dcfc8ce6cd |
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| Source note | uspto-grants-1985_04 |
|---|
