Hydrochloric Acid → HCID 20400419, compound

Participants

Reaction Conditions

Reaction Steps

The thus-obtained 2-(2,3,4-triacetoxybenzoyl)-3-oxobutanoate (3.2 g) was taken up in a mixture of tetrahydrofuran (160 ml) and 3N-HCl (160 ml) and agitated at 70° C. for 20.5 hours. The reaction mixture was concentrated to 20 ml and the resulting precipitate was collected by filtration. It was washed with water and then dried to give the desired product (0.94 g).

Provenance & Evidence