HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 2-(1-benzylpyrrolidin-3-yl)acetate → Methyl 2-(pyrrolidin-3-yl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 2-(1-benzylpyrrolidin-3-yl)acetate | HCID 4287640 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Methyl 2-(pyrrolidin-3-yl)acetate | HCID 13424175 | — |
Reaction Steps
The above prepared methyl 1-benzyl-3-pyrrolidineacetate hexamate was reduced in three portions, using 3.9 g. of 10% palladium on carbon in 200 ml. of absolute ethanol, for one hour at 50° C. The reaction mixture was filtered and concentrated to give methyl 3-pyrrolidineacetate hexamate, m.p. 68.5°-69.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04514414 |
| Source dataset | uspto-grants-1985_04 |
| ORD ID | ord-602380c5ea2d4a12abe6184b0d009ee8 |
| Source note | uspto-grants-1985_04 |