HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylhydrazine → 1-amino-3-(4-chlorophenyl)-1-methylthiourea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylhydrazine | HCID 6061 | — |
| Reactant | 4-Chlorophenyl isothiocyanate | HCID 16480 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-amino-3-(4-chlorophenyl)-1-methylthiourea | HCID 2060916 | — |
Reaction Steps
A mixture of 4-chlorophenylisothiocyanate (17.0 g, 0.10 mole) and methylhydrazine (5.0 g, 0.11 mole) in 80 ml of ethanol was stirred at room temperature for two hours. The reaction mixture was filtered to collect colorless crystalline N-(4-chlorophenyl)-1-methylhydrazinecarbothioamide (18.4 g, mp 152°-154° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04514419 |
| Source dataset | uspto-grants-1985_04 |
| ORD ID | ord-6d4d2704efcb46fc958055c8e078625f |
| Source note | uspto-grants-1985_04 |