Diethyl Ether → HCID 13178449, compound

HRID 1981419Notes

Reaction equation

HRID 1981419 reaction equation
C(=O)([O-])[O-].CS(O)(=O)=O.C(OCC)C.CS(O)(=O)=O.[C:20]([O:28][C:29]1[CH:34]=[CH:33][C:32]([C:35](=[NH:37])[NH2:36])=[C:31]([CH3:38])[CH:30]=1)(=[O:27])[C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1>CO>[C:20]([O:28][C:29]1[CH:34]=[CH:33][C:32]([C:35](=[NH:36])[NH2:37])=[C:31]([CH3:38])[CH:30]=1)(=[O:27])[C:21]1[CH:22]=[CH:23][CH:24]=[CH:25][CH:26]=1

Participants

6

Reactant 4

HCID 3283Diethyl EtherHCID 6395Methanesulfonic AcidHCID 19660Carbonate IonHCID 86740070HCID 86740070, compound

Product 1

HCID 13178449HCID 13178449, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The above carbonate was suspended in methanol and admixed with 60 mg of methanesulfonic acid. Upon addition of ethyl ether, there were obtained 160 mg of a white powder of 4-amidino-3-methylphenyl benzoate methanesulfonate.

Sources & evidence

ORD record
ord-ce48a03d459645f892228147cecab038
Source dataset
uspto-grants-1985_04
Patent number
US04514416

Reaction notes

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