HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 136387260, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Benzonitrile, 3-chloro-4-hydroxy- | HCID 2735739 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 136387260 | HCID 136387260 | — |
Reaction Steps
While being cooled in ice, a solution of 4.5 g of 2-chloro-4-cyanophenol in 50 ml of methanol was saturated with dried gaseous hydrogen chloride (HCl). The solution was left standing overnight at room temperature and mixed with 100 ml of ethyl ether to precipitate crystals which were collected by filtration to obtain 4.0 g of 2-chloro-4-methoxyiminomethylphenol hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04514416 |
| Source dataset | uspto-grants-1985_04 |
| ORD ID | ord-029196f52b4847e39996f8baf00ee086 |
| Source note | uspto-grants-1985_04 |