HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → 4-Amidino-2-benzoylphenol methanesulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | HCID 135598740 | HCID 135598740 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-Amidino-2-benzoylphenol methanesulfonate | HCID 54099182 | — |
Reaction Steps
In 200 ml of methanol, was suspended the 4-amidino-2-benzoylphenol hydrochloride obtained above. To the suspension was added 60 g of methanesulfonic acid followed by ethyl ether. The precipitated pale yellow crystals were collected by filtration and dried to obtain 109 g of 4-amidino-2-benzoylphenol methanesulfonate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04514416 |
| Source dataset | uspto-grants-1985_04 |
| ORD ID | ord-1e1056bd713c4b1dae1f0e2230923552 |
| Source note | uspto-grants-1985_04 |