HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → α-Phenyl-2-benzothiazolemethanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 23318519 | HCID 23318519 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | α-Phenyl-2-benzothiazolemethanamine | HCID 13342005 | — |
Reaction Steps
The hydrochloride was stirred with aqueous ammonia and methylene chloride, and the aqueous layer was extracted with two portions of methylene chloride. The combined methylene chloride extracts were washed with brine, dried over Na2SO4, filtered and concentrated in vacuo. 13.1 g of white solid, as desired product, was obtained, mp. 68°-70° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04592774 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-5808603c1b1743d2b9708677bca3ab96 |
| Source note | uspto-grants-1986_06 |