Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1981472Generated: November 2, 2026

4-Aminobenzoic Acid → HCID 13326883, compound

https://huagongshe.com/reaction/1981472

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Aminobenzoic AcidHCID 978—
ReactantTolueneHCID 1140—
ReactantHCID 13326882HCID 13326882—
ProductHCID 13326883HCID 13326883—

Reaction Conditions

Temperature0 °C

Reaction Steps

A 5.1 g. portion of 2,2-dihydroxy-1-[(3-phenoxy)phenyl]ethanone and 2.75 g. of p-aminobenzoic acid in 40 ml. of toluene was refluxed under argon for one hour, then cooled and evaporated to dryness. The residue was added to 40 ml. of ethanol and refluxed for 30 minutes, then cooled to 0° C., giving the desired product, m.p. 117°-127° C. (dec.).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04592876
Source datasetuspto-grants-1986_06
ORD IDord-01e14b9ccc2c48a29fc792f6cf13cc35
Source noteuspto-grants-1986_06