HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetaldehyde → HCID 13326884, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetaldehyde | HCID 177 | — |
| Reactant | 4-Aminobenzoic Acid | HCID 978 | — |
| Reactant | HCID 88674768 | HCID 88674768 | — |
| Product | HCID 13326884 | HCID 13326884 | — |
Reaction Steps
A mixture of 4.2 g. of 2,2-dihydroxy-4-(4-chloro-1-naphthyloxy)-α-oxo-benzeneacetaldehyde hemihydrate, 1.76 g. of p-aminobenzoic acid and 30 ml. of absolute ethanal was refluxed overnight under argon. The solid was collected, boiled in ethanol, cooled and filtered, giving the desired product as a pale yellow solid, m.p. 155°-165° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04592876 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-0584c366d8e045b9a5e3bf8079abbc21 |
| Source note | uspto-grants-1986_06 |