HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 23319717, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Phosgene | HCID 6371 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | 3-(3-Chloroanilino)butanoic acid | HCID 23319711 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 23319717 | HCID 23319717 | — |
Reaction Steps
7-Chloro-1-chloroformyl-2-methyl-1,2,3,4-tetrahydro-4-quinolinone is prepared in a manner similar to that described in Example 5 but starting from 3-(3-chloroanilino)butanoic acid (5.42 g; 25.4 mmol), phosgene (6.7 g; 67.7 mmol), methylene chloride (25 cc), dimethylformamide (0.23 cc) and aluminum chloride (8.15 g; 61.1 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04593101 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-a4949f01f22c4e8ea890fa73bb318e24 |
| Source note | uspto-grants-1986_06 |