HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloroaniline → 3-(3-Chloroanilino)butanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloroaniline | HCID 7932 | — |
| Reactant | Crotonic Acid | HCID 637090 | — |
| Product | 3-(3-Chloroanilino)butanoic acid | HCID 23319711 | — |
Reaction Steps
3-(3-Chloroanilino)butanoic acid is prepared in a manner similar to that described in Example 1, but starting from 3-chloroaniline (65 cc; 0.5 mol), crotonic acid (11.20 g; 0.129 mol) and distilled water (31 cc). After purification, a product (14.66 g; 68.6 mmol) is thus obtained in the form of a white powder which melts at about 50° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04593101 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-f5568cbecb4d4b1cb1cda7ac947b2d4e |
| Source note | uspto-grants-1986_06 |