HRID1981600
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
3-(3-Chloroanilino)butanoic acid is prepared in a manner similar to that described in Example 1, but starting from 3-chloroaniline (65 cc; 0.5 mol), crotonic acid (11.20 g; 0.129 mol) and distilled water (31 cc). After purification, a product (14.66 g; 68.6 mmol) is thus obtained in the form of a white powder which melts at about 50° C.
WORKUP
后处理
- distillationdistilled water (31 cc)
- customAfter purification
- customa product (14.66 g; 68.6 mmol) is thus obtained in the form of a white powder which melts at about 50° C.