HRID1981600

反应详情

EQUATION

反应方程式

HRID 1981600 的结构方程式

PROCEDURE

实验过程

3-(3-Chloroanilino)butanoic acid is prepared in a manner similar to that described in Example 1, but starting from 3-chloroaniline (65 cc; 0.5 mol), crotonic acid (11.20 g; 0.129 mol) and distilled water (31 cc). After purification, a product (14.66 g; 68.6 mmol) is thus obtained in the form of a white powder which melts at about 50° C.

WORKUP

后处理

  1. distillationdistilled water (31 cc)
  2. customAfter purification
  3. customa product (14.66 g; 68.6 mmol) is thus obtained in the form of a white powder which melts at about 50° C.