HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2-acetamido-3-benzylaminobutyrate → Ethyl 2-acetamido-3-aminobutyrate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2-acetamido-3-benzylaminobutyrate | HCID 13592826 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Ethyl 2-acetamido-3-aminobutyrate | HCID 23319786 | 100% |
Reaction Steps
Five grams of ethyl 2-acetamido-3-benzylaminobutyrate were dispersed in 20 ml of ethanol together with 0.5 of 5% palladium-on-carbon and shaken under 40 psi of hydrogen until hydrogen uptake had ceased. The mixture was filtered through Celite and evaporated to give a 100% yield of ethyl 2-acetamido-3-aminobutyrate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04593118 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-1240d6c20d4641eaaaa2a6f34dded9c5 |
| Source note | uspto-grants-1986_06 |