HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxynaphthalene → HCID 23319837, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxynaphthalene | HCID 7119 | — |
| Reactant | Diketene | HCID 12661 | — |
| Solvent | Hydrofluoric Acid | HCID 14917 | — |
| Product | HCID 23319837 | HCID 23319837 | 88% |
Reaction Steps
Eiglmeier, in U.S. 4,082,807, teaches the acylation of 2-methoxynaphthalene in anhydrous hydrogen fluoride with diketene to yield 1-acetoacetyl-2-methoxynaphthalene in 88% yield at -25° C. to -35° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04593125 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-72bab2b0945943a4ac05cb1a6c425f1f |
| Source note | uspto-grants-1986_06 |