Diethylamine → 2-[2-(Diethylamino)ethyl]-2,3-dihydro-4-methylpyrido[3,2-f][1,4]oxazepine-5(4H)-thione

HRID 1981736Notes

Reaction equation

HRID 1981736 reaction equation
Cl[CH2:2][CH2:3][CH:4]1[CH2:10][N:9]([CH3:11])[C:8](=[S:12])[C:7]2[CH:13]=[CH:14][CH:15]=[N:16][C:6]=2[O:5]1.[CH2:17]([NH:19][CH2:20][CH3:21])[CH3:18]>C(O)C>[CH2:17]([N:19]([CH2:20][CH3:21])[CH2:2][CH2:3][CH:4]1[CH2:10][N:9]([CH3:11])[C:8](=[S:12])[C:7]2[CH:13]=[CH:14][CH:15]=[N:16][C:6]=2[O:5]1)[CH3:18]

Participants

4

Reactant 2

HCID 8021DiethylamineHCID 137264422-(chloroethyl)-2,3-dihydro-4-methylpyrido[3,2-f]-1,4-oxazepine-5(4H)thione

Product 1

HCID 137265022-[2-(Diethylamino)ethyl]-2,3-dihydro-4-methylpyrido[3,2-f][1,4]oxazepine-5(4H)-thione

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

2-(2-Chloroethyl)-2,3-dihydro-4-methylpyrido[3,2-f][1,4]-oxazepine-5(4H)-thione and diethylamine in ethanol are heated together to obtain the title compound.

Sources & evidence

ORD record
ord-9b501176581d4ed7ac57d10bc0731d62
Source dataset
uspto-grants-1986_06
Patent number
US04592866

Reaction notes

Loading…