HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 13309451, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 13309444 | HCID 13309444 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 13309451 | HCID 13309451 | 82.2% |
Reaction Steps
16.6 g (0.1 mol) of methyl 2-(dimethylphosphinoyl)-2-hydroxyacetate are dissolved in 70 ml of methanol, which has first been gassed with NH3 gas for 10 minutes. After the mixture has been left to stand in a bomb tube at 25° for six days, it is filtered and concentrated and the oily residue is digested with ethyl acetate. 12.4 g (82.2%) of the amide of melting point 155° are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04594098 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-d3f5cdc8507e457f9a06b65359b2e7d4 |
| Source note | uspto-grants-1986_06 |