HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Methyl-3-(o-nitrobenzyl)-1,2,4-triazole → HCID 23317337, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Methyl-3-(o-nitrobenzyl)-1,2,4-triazole | HCID 13926284 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23317337 | HCID 23317337 | — |
Reaction Steps
A mixture of 1.67 g of 5-methyl-3-(o-nitrobenzyl)-1,2,4-triazole, 42 mg of 10% palladium on charcoal and 15 ml of ethanol is hydrogenated at 3 atmospheres pressure for 4 hours, filtered, decolorized, evaporated to a small volume and diluted with ether to give 3-(o-aminobenzyl)-5-methyl-1,2,4-triazole, m.p. 143°-145°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04595535 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-0ca15b9698c542778be6dfcca25b89c6 |
| Source note | uspto-grants-1986_06 |