HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Carbonyldiimidazole → HCID 54437824, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | HCID 178503406 | HCID 178503406 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 54437824 | HCID 54437824 | — |
Reaction Steps
A mixture of 7 g of 3-(o-aminobenzyl)-5-methylmercapto-1,2,4-triazole, 5.26 g of 1,1'-carbonyldiimidazole and 179 ml of methylene chloride is heated at reflux overnight. Most of the solvent is removed in vacuo, the solids are filtered and washed with small amount of methylene chloride to give 2-methylmercapto-11H-1,2,4-triazolo[2,3-c][1,3]benzodiazepine-5(6H)-one, m.p. 250°-252° (intermediate 5/b).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04595535 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-995b2c25d5db4e6fbabf38ef6b7321d1 |
| Source note | uspto-grants-1986_06 |