HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Methyl-3-(o-isothiocyanatobenzyl)-1,2,4-triazole → HCID 23317323, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Methyl-3-(o-isothiocyanatobenzyl)-1,2,4-triazole | HCID 23317336 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 23317323 | HCID 23317323 | — |
Reaction Steps
A suspension of 8 g of 5-methyl-3-(o-isothiocyanatobenzyl)-1,2,4-triazole in 100 ml of toluene is refluxed overnight and cooled to room temperature to give 2-methyl-11H-1,2,4-triazolo[2,3-c][1,3]-benzodiazepine-5(6H)-thione. Treatment with methyl iodide as described above yields 2-methyl-5-methylthio-11H-1,2,4-triazolo[2,3-c][1,3]benzodiazepine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04595535 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-d379b32ace21402c9fc99255a5407147 |
| Source note | uspto-grants-1986_06 |