Diphenylphosphine → HCID 14007796, compound

Participants

Reaction Steps

The vinyl tripropyl silane was then reacted with diphenyl phosphine with u.v. initiation for 86 hours in a manner described in Example 1. The conversion was about 95%. The mixture was fractionally distilled to yield approximately 63% of the theoretical yield of the product as a clear, colorless, mobile liquid. The product distilled at 155°-156° C. at 0.10 mm.

Provenance & Evidence