HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13645890, compound → HCID 14203029, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13645890 | HCID 13645890 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 14203029 | HCID 14203029 | 106.3% |
Reaction Steps
In 140 ml of ethyl acetate, 5.595 g of 1-(2,3-epoxypropyloxy)-2-benzyloxy-3,4-dichlorobenzene is hydrogenated under atmospheric pressure using 1.65 g of 5% palladium on carbon (50% moisture) as catalyst (for 20 minutes, 625 ml of hydrogen gas is absorbed.). After the catalyst is filtered off, the filtrate is evaporated to give 4.3 g of 1-(2,3-epoxypropyloxy)-2-hydroxy-3,4-dichlorobenzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04595767 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-d4bc558cffe04c2cbdfda504c172827b |
| Source note | uspto-grants-1986_06 |