反应详情

Utilizing the apparatus of Examples 1-5, 50 millimoles of sodium chloride, 100 millimoles of tri-n-octylaluminum, and 73 millimoles of tetrachlorosilane were reacted for 4 hours at 180° C. The analysis utilized in Examples 1-5 revealed that 62.9 mole percent tetraoctylsilane and 6.8 mole percent trioctylchlorosilane were produced based on tetrachlorosilane as the limiting reagent.

1. customwere reacted for 4 hours at 180° C