HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Chloride → Chloro(trioctyl)silane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Chloride | HCID 5234 | — |
| Reactant | Silicon tetrachloride | HCID 24816 | — |
| Reactant | HCID 620432 | HCID 620432 | — |
| Reactant | Tri-n-octylaluminum | HCID 16682948 | — |
| Product | Chloro(trioctyl)silane | HCID 13085273 | — |
Reaction Steps
Utilizing the apparatus of Examples 1-5, 50 millimoles of sodium chloride, 100 millimoles of tri-n-octylaluminum, and 73 millimoles of tetrachlorosilane were reacted for 4 hours at 180° C. The analysis utilized in Examples 1-5 revealed that 62.9 mole percent tetraoctylsilane and 6.8 mole percent trioctylchlorosilane were produced based on tetrachlorosilane as the limiting reagent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04595777 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-264d9c26b35e40e6863acd2018bb020b |
| Source note | uspto-grants-1986_06 |