HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 5,6,7,8-Tetrahydronaphthyl-N-methyl-N-(N'-methyl-N'-fluoroformylaminosulfenyl)carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 5,6,7,8-Tetrahydro-1-naphthol | HCID 68258 | — |
| Reactant | bis-(N-methyl-N-fluorocarbonylamino)sulfide | HCID 12897270 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 5,6,7,8-Tetrahydronaphthyl-N-methyl-N-(N'-methyl-N'-fluoroformylaminosulfenyl)carbamate | HCID 131714717 | — |
Reaction Steps
5,6,7,8-Tetrahydronaphthyl-N-methyl-N-(N'-methyl-N'-fluoroformylaminosulfenyl)carbamate was prepared by the procedure of Example IX by reacting 9.21 g of bis-(N-methyl-N-fluorocarbonylamino)sulfide with 7.41 g of 5,6,7,8-tetrahydro-1-naphthol in 300 ml of toluene with 5.05 g of triethylamine as acid acceptor to yield 9.5 g of an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04595769 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-ee01cffc346640c8b8a5bb26def1ce3d |
| Source note | uspto-grants-1986_06 |