Carbon Dioxide → HCID 178501445, compound

Participants

Reaction Steps

380 mg of Z-Sta-Sar-His-Lys(Boc)-OMe in 10 ml of 95% strength MeOH are hydrogenated with CO2 -absorption until saturation after the addition of 100 mg of Pd-on-carbon (10% Pd), the solution is filtered and concentrated to dryness. After drying in a high vacuum, H-Sta-Sar-His-Lys(Boc)-OMe is obtained in the form of an amorphous powder; Rf (G)=0.18; Rf (E)=0.53.

Provenance & Evidence