HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178514013, compound → HCID 178511197, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178514013 | HCID 178514013 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol--water (1/1) | HCID 22242641 | — |
| Product | HCID 178511197 | HCID 178511197 | — |
Reaction Steps
8.19 g of Z-β-Ala-His-NH2 are hydrogenated at room temperature under normal pressure for 15 hours in 200 ml of methanol/water (95:5) with 0.82 g of palladium-on-carbon (5% Pd). After filtering off the catalyst, evaporating off the solvent and drying, H-β-Ala-His-NH2 is obtained in the form of a colourless powder; Rf (L)=0.01.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04595677 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-a7e0ffbbb2ba4304b63c6f27345bb5f0 |
| Source note | uspto-grants-1986_06 |