HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Bromide → 6,11-Dihydro-11-hydroxydibenz[b,e]oxepin-2-carbonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Bromide | HCID 253877 | — |
| Reactant | 2-Cyano-6,11-dihydro-11-oxodibenz[b,e]oxepin | HCID 12446825 | — |
| Product | 6,11-Dihydro-11-hydroxydibenz[b,e]oxepin-2-carbonitrile | HCID 54117505 | — |
Reaction Steps
In a similar manner as above, 6,11-dihydro-11-hydroxydibenz[b,e]oxepin-2-carbonitrile XII was prepared from the oxepin-carbonitrile XI in a quantitative yield. IR spectrum (KBr tablet, cm-1): 2230, 1610, 1500, 1260, 1240, 1000; NMR spectrum (CDCl3 +d6DMSO, δ-value, ppm): 5.23(d, 1H), 5.72(d, 1H), 5.88(d, 1H), 6.15(d, 1H), 6.7-7.9(m, 7H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04596804 |
| Source dataset | uspto-grants-1986_06 |
| ORD ID | ord-11276c911d5444238e83b31765168872 |
| Source note | uspto-grants-1986_06 |