HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1982448Generated: November 1, 2026
Dimethylformamide dimethyl acetal → HCID 23316511, compound
https://huagongshe.com/reaction/1982448
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | 9H-beta-Carboline-3-carboxamide | HCID 13129465 | — |
| Product | HCID 23316511 | HCID 23316511 | — |
Reaction Steps
A mixture of 1.0 g of beta-carboline-3-carboxamide and 3 ml of dimethyl-formamide-dimethylacetal is heated for 3 h at about 115° C. in an oil bath. After cooling, the crystals are collected on a glass frit and washed with 1 ml of dimethylformamide and then with 20 ml of ether. 1.2 g of N-[(dimethylamino)methylene]-beta-carboline-3-carboxamide with a m.p. of 307°-317° C. is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04596808 |
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| Source dataset | uspto-grants-1986_06 |
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| ORD ID | ord-c5d22185377c45d58f14e08a9f2595f6 |
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| Source note | uspto-grants-1986_06 |
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